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Beilstein J. Org. Chem. 2016, 12, 1758–1764, doi:10.3762/bjoc.12.164
Graphical Abstract
Scheme 1: Iterative synthesis of trisaccharide 66.
Scheme 2: Proposed mechanisms for TMSBr-mediated synthesis of 2-deoxyglycosides in the presence of TPPO.